Baixe no formato pdf, txt ou leia online no scribd. Combining the coulometric technique with karl fischer titration, aquamax kf titrators determine the water content of the sample by measuring the amount of electrolysis current necessary to produce the. Determination of water content according to karl fischer direct method. Application news, practical tips for the laboratory, and more. New pyridinefree kf reagents use amines and glycol ethers to replace the pyridine and methanol. User guide read online or download pdf metrohm 756 kf coulometer user manual metrohm equipment. Karl fischer titration introduction to karl fischer titration 36 volumetric kf titrators 37 volumetric kf titrators overview 37 890901 titrando 38 915 kf titouch 39 870 kf titrino plus 40 kf coulometer 41 coulometric kf titrators overview 41 851852 titrando 42 756 831 kf coulometer 43 899 coulometer 44 manual kf. Connecting metrohm rs232 interface to sartorius balance. More catalogs by metrohm ag 831 kf coulometer 8 pages. Notice demploi lire en ligne ou telecharger en pdf metrohm 756 kf coulometer manuel dutilisation equipement metrohm. In combination with a 774 oven sample processor, the 831 kf coulometer can be expanded to a fully automated analysis system. Rinse the syringe by turning it round and holding the needle point. In this way you have all the features and advantages of. Karl fischer moisture titrator coulometric titration mkc710m large color tftlcd with a touch panel 8.
Application bulletin 2801 e automated karl fischer water. Disassembly looks very complex, especially when the problem is with the carousel but once you have an understanding of the mechanism its not that difficult. The karl fischer titration anthony lucio the university of iowa shaw group meeting. The traditional kf reagent contains iodine, sulfur dioxide in pyridine and methanol. We have 1 mettler toledo dl39 manual available for free pdf download.
Robert leitner we provide manuals to wide mznual of devices, including. Karl fischer coulometric titration explained and illustrated noria corporation in some industries and environments, water is a far more damaging contaminant than solid particles and is often overlooked as a primary cause of component failure. Water determination by karl fischer titration agnieszka kossakowska praha, 03. Economical kf coulometer with diaphragmless titration cell for water determination right down to trace levels. Karl fischer titration, karl fischer method, coulometric. Inexpensive coulometer including titration cell and generator electrode with diaphragm for water content determination down to trace levels. Karl fischer titration introduction to karl fischer titration 36 volumetric kf titrators 37 volumetric kf titrators overview 37 890901 titrando 38 915 kf titouch 39 870 kf titrino plus 40 kf coulometer 41 coulometric kf titrators overview 41 851852 titrando 42 756 831 kf coulometer 43 899 coulometer 44 manual kf sample preparation 45. Instructions for use 756 831 kf coulometer, english english pdf metrohm newsletter register now. The amount of current required to convert the water is the determinant of the amount of moisture. Despite its exceptionally favorable price, the youngest member of our karl fischer instrument range leaves no wish unfulfilled. Operating instructions mettler toledo dl37 kf coulometer. As shown in formula 1 below, the karl fischer method uses karl fischer reagent, which reacts quantitatively and selectively with water, to measure moisture content. This inexpensive, timetested coulometric titrator allows you to analyze samples with low water contents 0.
High sample throughputs are best dealt with by the fully automated 774 oven sample processor. Thus, it can be linked to a manual oven 860 kf thermoprep or to an 885 compact oven sample changer for fully automated thermal sample preparation and subsequent coulometric. With the mettler dl37 kf coulometer you can easily determine traces of water with a very high degree of accuracy. This inexpensive, timetested coulometric titrator allows you to analyse samples with low water contents 0. Validation report and uncertainty budgetof coulometric karl fischer. Jun 24, 2019 hp officejet 6310 allinone manual pdf find support and troubleshooting info including software, drivers, and manuals for your hp officejet allinone printer. The remote interface opens up further possibilities.
Metrohm coulometric karl fischer titration youtube. Kf titrino coulometer the 756 and 831 coulometers have gained a reputation for dependability and accuracy. You can make a request for the operating manual by completing the adjoining form. View and download advanced 3320 service manual online. During the determination the iodide is oxidized to iodine at the anode of the generator electrode. It can download results directly from the titrator through a serial port connection, or open result files previously saved to disk the results manager package contains all necessary cables, connections, installation cd and user manual. The 831 kf coulometer is equipped with two rs 232c interfaces that allow the attachment of a balance, printer and pc. The aqc34 is optimized for simple routine determinations. When a sample is introduced into the titration cell and dissolved, reagent is released by the induction of an electrical current. About this document this document provides you with the information you need to get started with your mettler toledo titrator. The favorably priced 870 kf titrino plus is metrohms new karl fischer titrator for. A coulometric karl fischer instrument is often referred to as a coulometer.
Metrohm 756 kf coulometer user manual page 106 163. The coulometer is connected to a computer by way of one of the rs232 interfaces. Validation report and uncertainty budgetof coulometric karl. In this way you have all the features and advantages of tiamotm available to you.
Inexpensive coulometer including titration cell with generator electrode without diaphragm for water content determination down to trace levels. Metrohms 831 kf coulometer sets new standards regarding priceperformance ratio. Procedure for 831 kf coulometer immediately after breaking open the corresponding vial, fill the syringe about half with the standard solution. User guide read online or download pdf metrohm 756 kf coulometer user. Coulometric water content determination according to karl fischer. Mount the coulometer cell as follows on a titration stand. These inexpensive, timetested coulometric titrators allow you to analyze samples with low. Karl fischer reagent consists of iodine, sulfur dioxide, a base and a sol.
We supply a wide range of brand new equipment for the laboratory ph, petroleum product testers, freezers, furnaces, microscopes and more. Instructions for use 756 831 kf coulometer, english. Oil titouch allinclusive package for the nonaqueous acidbase titration of oil products food titouch allinclusive package for aqueous acidbase titration in foodstuffs, etc. The 831 kf coulometer guarantees precise and accurate results even in the low microgram region. The lcd screen shows what is happening in the titration cell at all times. The third functions inscriptions in the triangle on the keys of the. For a coulometric karl fischer titration a modified kf reagent which contains iodide is used. Karl fischer kf determination of water with kf drying. Metrohm accessories and replacement parts for models 756. Water is quantified from the volume of kf reagent consumed 100 to 1x106 ppm 0. They are identical for a 831 kf coulometer, except from the instrument number. Karl fischer coulometric titration explained and illustrated. Thank you for choosing a mettler toledo coulometric kf titrator. This coulometer has become indispensable in many laboratories thanks to its reliability, its backlit graphical display, the multilanguage dialog and the simplicity of its operation.
Functions, which only apply on the 756 kf coulometer are marked accordingly. Subsequently, you will receive the operating manual as pdf. With the dl37 you have the possibility to adapt the titration parameters control gain, end point indication, etc. The coulometric karl fischer titration is concerned with the determination of traces of water from e. Instructions for use 756831 kf coulometer, english english. Read online or download pdf page 106 163 metrohm 756 kf coulometer user manual metrohm equipment. With dimensions of 144 x 112 x 282 mm w x h x d the new metrohm coulometer.
Generation of forgeproof pdf reports without a pc yes usb flash drive for saving methods. The iodine in the presence of water is reduced to colorless hydrogen iodide. Karl fischer moisture titrator coulometric method features optional accessories specification features specification nonce conformance the model adp511s evaporator can be used in conjunction with. The clear display provides information regarding the relevant. The coulometric kf titrator is an easytooperate instrument for coulometric karl fischer titrations. Metrohm 831 kf coulometer for measurement of water content by means of karl fischer titration method. At the same time, the 899 coulometer provides the capabilities of a fullgrown metrohm coulometer. Inject part of the standard solution with one stroke. Metrohm 756 kf coulometer user manual 5 mode selection, key. If this is not possible, then you should reset all processrelated settings under config to the default values autostart off, silo off, start delay off, all monitoring to. Metrohm 831 kf coulometer kf coulometer lambdaelan.
The karl fischer oven technique for the easy preparation of difficult samples. Metrohm accessories and replacement parts for models 756 and 831 kf coulometers. Alternatively, the 756 831 coulometer can be controlled with tiamotm software. You can find a short summary of the instructions for use in the enclosed 756 831 kf coulometer. The basics of karl fischer titration karl fischer titration is an analytical technique to measure the amount of water contained in various samples, which may be solid, liquid or gaseous. The dl32 type coulometer, presented in figure 9, appendix 3, is a microprocessorcontrolled analytical instrument working in the range of 150 000 g h 2 o g. You can find a short summary of the instructions for use in the enclosed 756 831 kf coulometer quick references. How should the titrino and the 756 831 kf coulometer be set so that the equipment works perfectly with tiamo. The 831 coulometer has gained a reputation for dependability and accuracy. Oil test laboratoryrev 01 bharat heavy electricals. Metrohm 756 kf coulometer manuel dutilisation pages. The 756 and 831 kf coulometers for water content determinations in the trace region.